Studying the Optimum Conditions for the Synthesis the Derivatives of Salicylaldehyde with Halides Compounds
Journal of Biomaterials
Volume 1, Issue 2, December 2017, Pages: 34-39
Received: Apr. 8, 2017;
Accepted: May 22, 2017;
Published: Jul. 13, 2017
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Joumaa Merza, Department of Chemistry, Faculty of Sciences, Al-Baath University, Homs, Syria
Ali Alasmi, Department of Chemistry, Faculty of Sciences, Al-Baath University, Homs, Syria
Three Dialdehydes were synthesized by the reaction of Salicylaldehyde and many Aliphatic and Aromatic Halides. The optimal condition (Catalysts, Temperature, Time of Reaction and Effect of Solvents) to get a high selective compounds and high yields have been studied. The reactions were followed by using Thin Layer Chromatography (TLC). The synthesized compounds were purified and characterized by means of High Performance Liquid Chromatography (HPLC) and spectroscopy methods: Infrared Spectra (IR), 1 H-NMR, 13C-NMR.
Studying the Optimum Conditions for the Synthesis the Derivatives of Salicylaldehyde with Halides Compounds, Journal of Biomaterials.
Vol. 1, No. 2,
2017, pp. 34-39.
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