Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar
Science Journal of Analytical Chemistry
Volume 8, Issue 1, March 2020, Pages: 5-11
Received: Dec. 21, 2019;
Accepted: Jan. 8, 2020;
Published: Jan. 31, 2020
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Qiang Sun, Agonomy College, Heilongjiang Bayi Agricultural University, Daqing, China
Yuliang Gao, Agonomy College, Heilongjiang Bayi Agricultural University, Daqing, China
Liyan Wang, Agonomy College, Heilongjiang Bayi Agricultural University, Daqing, China
A simple, efficient and environmentally friendly method has been established for the analysis of organic components in wood vinegar (WV) by dispersive liquid-liquid micro-extraction based on solidification of floating organic droplet (DLLME-SFO) coupled with GC/MS. Several variables that affect the extraction efficiency, including the type and volume of the extractant and dispersant, extraction time and the mass fraction of sodium chloride were optimized. Under the optimum conditions, the sample extracted were analyzed by GC/MS. The result shows that, apart from the main component of acetic acid, many kinds of ketone compound, phenol compound, ester compound, aldehyde and alcohol compound exist in the WV. The proposed method has been successfully employed to determine the organic components in the WV.
Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar, Science Journal of Analytical Chemistry.
Vol. 8, No. 1,
2020, pp. 5-11.
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